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Sampling, preparation and treatment of sea samples : statistical approaches


  • N. Nassif 1, R. Saliba2, G. Khalaf 1, C. Ducauze3
  • 1 Centre National des Sciences Marines - CNRS - Liban
  • 2 Université Libanaise - Faculté d’Agronomie
  • 3 Institut National Agronomique Paris-Grignon
  • The Regional Workshop on Marine Sciences & Natural Resources 25-26 May 2004.

Abstract


In the analytical pathway, from the elementary sampling to the analytical result, the sampling, the preparation of a laboratory sample and the treatment of the test sample represent two critical steps for any analytical method. We discussed the example of sea sediments.

Having performed a variance analysis, we demonstrate that the contribution of the analysis (treatment and instrumental mesure) represents a small part of the variance, the most important part coming from the heterogeneity of the analytes in the samples. Attention must be paid to the preparation of the laboratory sample.

Key words: environmental samples, sampling, heterogeneity, metals, variance.


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